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US Patent 8163786 Preparation of a lead-free primary explosive

Patent 8163786 was granted and assigned to Pacific Scientific Energetic Materials Company on April, 2012 by the United States Patent and Trademark Office.

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Patent
Patent
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Patent attributes

Current Assignee
Pacific Scientific Energetic Materials Company
Pacific Scientific Energetic Materials Company
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Patent Jurisdiction
United States Patent and Trademark Office
United States Patent and Trademark Office
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Patent Number
81637860
Patent Inventor Names
Michael D. Williams0
John W. Fronabarger0
Date of Patent
April 24, 2012
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Patent Application Number
126918490
Date Filed
January 22, 2010
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Patent Primary Examiner
‌
Susannah Chung
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Patent abstract

Embodiments of the present subject matter provide a compound and material that may be used as a lead-free primary explosive. An embodiment of the present subject matter provides the compound copper(I) nitrotetrazolate. Certain embodiments of the present subject matter provide methods for preparing lead-free primary explosives. The method includes: providing a cupric salt; providing water; providing a 5-nitrotetrazolate salt; combining the cupric salt, water and 5-nitrotetrazolate salt to form a mixture, heating the mixture, adding a reducing agent and stirring with continued heating. The method may also include providing cupric chloride, sodium 5-nitrotetrazolate and sodium ascorbate. Certain embodiments of the present subject matter also provide methods for preparing copper(I) nitrotetrazolate. The method includes: providing cupric salt; providing water; providing 5-nitrotetrazolate salt; combining the cupric salt, water and 5-nitrotetrazolate salt to form a mixture, heating the mixture, adding a reducing agent and stirring with continued heating. The method may also include providing cupric chloride, sodium 5-nitrotetrazolate and sodium ascorbate.

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