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US Patent 7915893 NMR CryoMAS probe for high-field wide-bore magnets

Patent 7915893 was granted and assigned to Doty Scientific on March, 2011 by the United States Patent and Trademark Office.

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Current Assignee
Doty Scientific
Doty Scientific
Patent Jurisdiction
United States Patent and Trademark Office
United States Patent and Trademark Office
Patent Number
7915893
Date of Patent
March 29, 2011
Patent Application Number
12518946
Date Filed
November 18, 2007
Patent Primary Examiner
‌
Brij B. Shrivastav
Patent abstract

All critical circuit components, including the sample coils, are located along with the spinner assembly in a region that may be evacuated to high vacuum for thermal insulation and high-voltage operation. A hermetically sealed spinner assembly simultaneously satisfies the requirements of hermeticity, low total emissivity, rf compatibility, spinning performance, magnetic compatibility, and high filling factor by utilizing metal construction except for the central region near the rf sample coils. Hence, it is possible to maintain high vacuum in the region external to the MAS spinner assembly even over a broad range of bearing and drive gas temperatures. A bundle of optical fibers is provided for tachometry for spin rates up to 60 kHz. The use of alumina disc capacitors allows the noise contributions from the most critical capacitors to be reduced to a minor fraction of the total and simplifies high voltage operation.

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