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US Patent 11162040 Method for preparing low-sulfur biodiesel

Patent 11162040 was granted and assigned to Zhejiang University of Technology on November, 2021 by the United States Patent and Trademark Office.

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Patent Applicant
Zhejiang University of Technology
Zhejiang University of Technology
Current Assignee
Zhejiang University of Technology
Zhejiang University of Technology
Patent Jurisdiction
United States Patent and Trademark Office
United States Patent and Trademark Office
Patent Number
11162040
Date of Patent
November 2, 2021
Patent Application Number
20181228
Date Filed
December 28, 2018
Patent abstract

The present invention relates to a method for preparing low-sulfur biodiesel. The method includes the following steps: subjecting raw crude oil to heat exchange, preheating, glycerol esterification reaction, flashing, cooling, transesterification, dealcoholization, sedimentation, and methyl ester rectification to obtain low-sulfur biodiesel up to the standard, where in the heat exchange process, the raw crude oil exchanges heat with flashed oil to recycle some heat, and glycerol and fatty acids in a distilled product subjected to flashing are reused for the glycerol esterification reaction; the dealcoholization process removes methanol in a system after the transesterification, and refined methanol recycled by methanol rectification is reused for the transesterification reaction; crude glycerol generated in the sedimentation process does not need to be treated and is directly used for glycerol rectification to obtain refined glycerol, and the refined glycerol is reused for the glycerol esterification reaction.

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