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US Patent 10259725 Method of synthesizing cellulose nano-crystals from date palm seeds

Patent 10259725 was granted and assigned to United Arab Emirates University on April, 2019 by the United States Patent and Trademark Office.

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Patent
Patent
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Patent attributes

Patent Applicant
United Arab Emirates University
United Arab Emirates University
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Current Assignee
United Arab Emirates University
United Arab Emirates University
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Patent Jurisdiction
United States Patent and Trademark Office
United States Patent and Trademark Office
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Patent Number
102597250
Patent Inventor Names
Ruwaya Alkendi0
Victor Sagaya0
Date of Patent
April 16, 2019
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Patent Application Number
153963070
Date Filed
December 30, 2016
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Patent Citations Received
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US Patent 11772016 Date seed powder for water filtration treatment
Patent Primary Examiner
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Krishnan S. Menon
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Patent abstract

A method of synthesizing cellulose nano-crystals from date palm seeds includes providing washed and dried date palm seeds, milling the date palm seeds to a fine powder, adding a bleaching agent to the fine powder to separate cellulose from the powder, placing the cellulose in a container with an acid solution to form a mixture, heating the mixture, isolating cellulose crystals from the mixture, and reducing the particle size of the cellulose crystals in the solution to provide cellulose nano-crystals. The particle size can be reduced by adding the cellulose crystals to a quantity of water to form a solution, and ultrasonicating the solution at about 90% amplitude for about 45 minutes to form cellulose nano-crystals. The cellulose nano-crystals can have a size ranging from about 5 nm to about 100 nm.

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