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US Patent 7544626 Preparation of self-assembled silicon nanotubes by hydrothermal method

Patent 7544626 was granted and assigned to Hunan University on June, 2009 by the United States Patent and Trademark Office.

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Patent
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Patent attributes

Current Assignee
Hunan University
Hunan University
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Patent Jurisdiction
United States Patent and Trademark Office
United States Patent and Trademark Office
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Patent Number
75446260
Patent Inventor Names
Yuanhong Tang0
Chi Guo0
Lizhai Pei0
Yangwen Chen0
Date of Patent
June 9, 2009
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Patent Application Number
105784500
Date Filed
May 8, 2005
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Patent Primary Examiner
‌
David Vu
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Patent abstract

The present invention relates to a method for preparing self-assembled silicon nanotubes (SiNTs) by a hydrothermal method. A method for preparing self-assembled SiNTs comprises forming a mixture of silicon oxide and water in a sealed container, wherein the mixture has a silicon oxide to water ratio of no more than 10% by weight. The mixture is maintained at a constant temperature and a constant pressure, and the mixture is stirred for a period of time. Self-assembled SiNTs may be formed with an average inner diameter of less than 5 nm and an average outer diameter of around 15 nm. The present invention completely utilizes non-toxic raw materials, and the materials and process do not pollute the environment, so the method satisfies the development trends of the modern industry.

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